1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine

Base Information

• Chemical Name: 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine
• CAS No.: 154060-72-7
• Molecular Formula: C₂₃H₃₀N₂O₃
• Molecular Weight: 382.503

Synonyms:1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine

Chemical Property of 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine

Chemical Property:

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Technology Process of 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine

There total 4 articles about 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(chloromethyl)benzyl chloride (626-16-4) → 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine (154060-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 4 h / Heating

2: 18-crown-6 / acetonitrile / 4 h / Heating

With 18-crown-6 ether; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jm00021a010

Reference yield:

2-(1-methylethoxy)phenyl-1-piperazine (54013-91-1) → 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine (154060-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 4 h / Heating

2: 18-crown-6 / acetonitrile / 4 h / Heating

With 18-crown-6 ether; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jm00021a010

Reference yield:

potassium acetate (127-08-2) + 1-(3-Chloromethyl-benzyl)-4-(2-isopropoxy-phenyl)-piperazine (155106-81-3) → 1-<<3-(acetoxymethyl)phenyl>methyl>-4-<2-(1-methylethoxy)phenyl>piperazine (154060-72-7)

Guidance literature:

With 18-crown-6 ether; In acetonitrile; for 4h; Heating;

DOI:10.1021/jm00021a010

upstream raw materials:

potassium acetate

1-(3-Chloromethyl-benzyl)-4-(2-isopropoxy-phenyl)-piperazine

3-(chloromethyl)benzyl chloride

2-(1-methylethoxy)phenyl-1-piperazine

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