(E)-3-(2-methoxyphenyl)allyl pivalate

Base Information

Chemical Name:(E)-3-(2-methoxyphenyl)allyl pivalate
CAS No.:1014394-74-1
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:

Synonyms:(E)-3-(2-methoxyphenyl)allyl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(2-methoxyphenyl)allyl pivalate

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Technology Process of (E)-3-(2-methoxyphenyl)allyl pivalate

There total 3 articles about (E)-3-(2-methoxyphenyl)allyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1504-61-6,13523-28-9,114568-19-3
(E)-3-(2-methoxyphenyl)prop-2-en-1-ol

: 3282-30-2
pivaloyl chloride

: 1014394-74-1
(E)-3-(2-methoxyphenyl)allyl pivalate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 200 ℃; for 1.5h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0036-1590914

Reference yield:

: 3698-28-0
2-allylanisole

: 75-98-9
Trimethylacetic acid

: 1014394-74-1
(E)-3-(2-methoxyphenyl)allyl pivalate

: (Z)-3-(2-methoxyphenyl)allyl pivalate

Guidance literature:: Trimethylacetic acid; With lithium hydroxide monohydrate; at 40 ℃; for 0.166667h;

With manganese(IV) oxide; palladium diacetate; p-benzoquinone; In acetonitrile; at 20 ℃; for 0.25h;

2-allylanisole; In acetonitrile; at 40 ℃; for 72h; optical yield given as %de; stereoselective reaction;
DOI:10.1021/jo902587u

Reference yield:

: 1504-61-6
2-methoxycinnamyl alcohol

: 1538-75-6
2,2-dimethylpropanoic anhydride

: 1014394-74-1
(E)-3-(2-methoxyphenyl)allyl pivalate

: (Z)-3-(2-methoxyphenyl)allyl pivalate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; for 12h; Overall yield = 70 %; Overall yield = 870 mg; Inert atmosphere;
DOI:10.1021/jacs.6b10220