5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione

Base Information Edit

Chemical Name:5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione
CAS No.:1300031-69-9
Molecular Formula:C₁₄H₁₄INO₅
Molecular Weight:403.173
Hs Code.:
Mol file:1300031-69-9.mol

Synonyms:5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione

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Chemical Property of 5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione Edit

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Technology Process of 5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione

There total 4 articles about 5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.9%

: 2033-24-1
cycl-isopropylidene malonate

: 74587-12-5
3-iodo-4-methoxyaniline

: 149-73-5
trimethyl orthoformate

: 1300031-69-9
5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: cycl-isopropylidene malonate; trimethyl orthoformate; for 1h; Reflux;

3-iodo-4-methoxyaniline; for 1h; Reflux;

Reference yield:

: 5399-03-1
2-iodo-1-methoxy-4-nitrobenzene

: 1300031-69-9
5-{[(3-iodo-4-methoxyphenyl)amino]methylene}-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride; ethanol / water / 5 h / Reflux

2: ethanol / 2 h / Reflux

With ethanol; iron; ammonium chloride; In ethanol; water;