1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol

Base Information Edit

Chemical Name:1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol
CAS No.:1139-06-6
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:220.312
Hs Code.:
Mol file:1139-06-6.mol

Synonyms:1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol Edit

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Technology Process of 1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol

There total 9 articles about 1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 98-86-2
acetophenone

: 1139-06-6
1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol

Guidance literature:: cyclohexanone; acetophenone; With chloro-trimethyl-silane; magnesium; In N,N-dimethyl-formamide; at 20 ℃;

With sulfuric acid; In methanol; at 20 ℃; for 6h; Further stages.;
DOI:10.1016/j.tetlet.2004.03.109

Reference yield:

: 1139-06-6
1-hydroxy-α-methyl-α-phenyl-cyclohexanemethanol

Guidance literature:: With potassium hydrogensulfate; at 130 - 140 ℃; Behandeln des Reaktionsgemisches mit Peroxyameisensaeure in wss. Ameisensaeure und Erwaermen des danach erhaltenen Reaktionsprodukts mit wss.-aethanol. NaOH;
DOI:10.1021/ja01135a049