N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

Base Information

Chemical Name:N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide
CAS No.:1489231-07-3
Molecular Formula:C₁₅H₁₂N₆O₄S
Molecular Weight:372.364
Hs Code.:

Synonyms:N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

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Technology Process of N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

There total 3 articles about N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 76960-33-3
4-nitro-N-(4-oxocyclohexa-2,5-dien-1-ylidene)benzamide

: 13183-79-4
1-methyl-5-mercaptotetrazole

: 1489231-07-3
N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1016/j.ejmech.2013.07.056

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1489231-07-3
N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 5 h / 20 °C / Cooling with ice

2: SiO₂-supported NaIO₄ / dichloromethane / 2 h / 20 °C

3: N,N-dimethyl-formamide / 4 h / 20 °C

With SiO₂-supported NaIO₄; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3: |Michael Addition;
DOI:10.1016/j.ejmech.2013.07.056

Reference yield:

: 51-78-5
p-aminophenol hydrochloride

: 1489231-07-3
N-(4-hydroxy-3-((1-methyl-1H-tetrazol-5-yl)thio)phenyl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 5 h / 20 °C / Cooling with ice

2: SiO₂-supported NaIO₄ / dichloromethane / 2 h / 20 °C

3: N,N-dimethyl-formamide / 4 h / 20 °C

With SiO₂-supported NaIO₄; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3: |Michael Addition;
DOI:10.1016/j.ejmech.2013.07.056