Technology Process of 2-Propenoic acid, 2-methyl-, 11-8trimethoxysilyl)undecyl ester 2-Propenoic acid,2-methyl-,11-8trimethoxysilyl)undecyl ester
There total 2 articles about 2-Propenoic acid, 2-methyl-, 11-8trimethoxysilyl)undecyl ester 2-Propenoic acid,2-methyl-,11-8trimethoxysilyl)undecyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
undec-10-en-1-yl methacrylate;
With
2,6-di-tert-butyl-4-methyl-phenol; 1,3,5-trimethyl-2,4,6-tris-(3,5-di-tert-butyl-4-hydroxybenzyl)benzene; trichlorosilane;
dihydrogen hexachloroplatinate;
In
isopropyl alcohol; toluene;
methanol;
With
urea;
In
isopropyl alcohol; toluene;
at 50 ℃;
DOI:10.1246/bcsj.76.1441
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: p-TsOH*H2O / toluene / Heating
2.1: 1,3,5-Me3-2,4,6-tris(3,5-di-t-Bu-4-hydroxybenzyl)benzene; 2,6-di-t-butyl-4-methylphenol; HSiCl3 / H2PtCl6*6H2O / propan-2-ol; toluene
2.2: urea / propan-2-ol; toluene / 50 °C
With
2,6-di-tert-butyl-4-methyl-phenol; 1,3,5-trimethyl-2,4,6-tris-(3,5-di-tert-butyl-4-hydroxybenzyl)benzene; trichlorosilane; toluene-4-sulfonic acid;
dihydrogen hexachloroplatinate;
In
isopropyl alcohol; toluene;
DOI:10.1246/bcsj.76.1441
