(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

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Chemical Name:(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol
CAS No.:1459754-30-3
Molecular Formula:C₂₅H₃₁ClO₈
Molecular Weight:494.969
Hs Code.:

Synonyms:(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

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Chemical Property of (3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

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Technology Process of (3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

There total 5 articles about (3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.8%

: 67-56-1
methanol

: 1400980-44-0
1-chloro-2-(4-(2-cyclopropoxyethoxy)benzyl)-4-iodobenzene

: 32469-28-6,55515-28-1,55515-29-2,32384-65-9
(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one

: 1459754-30-3
(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: 1-chloro-2-(4-(2-cyclopropoxyethoxy)benzyl)-4-iodobenzene; With TurboGrignard; In tetrahydrofuran; at -60 - -50 ℃; for 1.25h; Inert atmosphere; Large scale;

(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one; In tetrahydrofuran; n-heptane; at -50 - -10 ℃; for 5.58333h; Inert atmosphere; Large scale;

methanol; With hydrogenchloride; water; In tetrahydrofuran; at -10 - 20 ℃; for 16h; Concentration; Temperature; Time; Large scale;

Reference yield:

: 67-56-1
methanol

: C₂₄H₂₉ClO₈

: 1459754-30-3
(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at -10 - 20 ℃; for 16h; Concentration; Temperature;

Reference yield:

: 67-56-1
methanol

: C₃₆H₆₁ClO₈Si₄

: 1459754-30-3
(3R,4S,5S,6R)-2-(4-chloro-3-(4-(2-cyclopropoxyethoxy)benzyl)phenyl)-6-(hydroxymethyl)-2-methoxytetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; hexane; water; toluene; at 20 - 25 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.09.003