C₁₁H₁₅NO₂*ClH

Base Information

Chemical Name:C₁₁H₁₅NO₂*ClH
CAS No.:1048653-48-0
Molecular Formula:C₁₁H₁₅NO₂*ClH
Molecular Weight:229.707
Hs Code.:

C<sub>11</sub>H<sub>15</sub>NO<sub>2</sub>*ClH

Synonyms:C₁₁H₁₅NO₂*ClH

Suppliers and Price of C₁₁H₁₅NO₂*ClH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₁H₁₅NO₂*ClH

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₁H₁₅NO₂*ClH

There total 2 articles about C₁₁H₁₅NO₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67-56-1
methanol

: (R)-(+)-α-4-methylphenylalanine

: 1048653-48-0
C₁₁H₁₅NO₂*ClH

Guidance literature:: methanol; (R)-(+)-α-4-methylphenylalanine; With thionyl chloride; at -15 ℃; Reflux;

With calcium carbonate; In water; ethyl acetate; at 20 ℃; for 2h;

With hydrogenchloride; In water; ethyl acetate;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 122-00-9
para-methylacetophenone

: 1048653-48-0
C₁₁H₁₅NO₂*ClH

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium hydroxide / ethanol / 4 h / 60 - 65 °C

1.3: Auto-seeded programmed polythermic preferential crystallization; Resolution of racemate

2.1: sodium hydroxide / water / 72 h / Reflux

3.1: thionyl chloride / -15 °C / Reflux

3.2: 2 h / 20 °C

With ammonium hydroxide; thionyl chloride; sodium hydroxide; In ethanol; water; 1.1: Bucherer-Bergs reaction;
DOI:10.1016/j.tet.2011.06.032

Reference yield: 93.0%

: 1048653-48-0
C₁₁H₁₅NO₂*ClH

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 888970-78-3
C₂₁H₂₄N₂O₅

Guidance literature:: C₁₁H₁₅NO₂*ClH; N-(Benzyloxycarbonyl)glycine; With HATU; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.032