C₂₅H₃₁N₃O₄S

Base Information

Chemical Name:C₂₅H₃₁N₃O₄S
CAS No.:1310731-57-7
Molecular Formula:C₂₅H₃₁N₃O₄S
Molecular Weight:469.605
Hs Code.:

C<sub>25</sub>H<sub>31</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:C₂₅H₃₁N₃O₄S

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Chemical Property of C₂₅H₃₁N₃O₄S

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Technology Process of C₂₅H₃₁N₃O₄S

There total 8 articles about C₂₅H₃₁N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1310731-56-6
C₂₅H₂₉N₃O₄S

: 1310731-57-7
C₂₅H₃₁N₃O₄S

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmcl.2012.11.108

Reference yield:

: 1310704-15-4
ethyl 4-chloro-1-(triisopropylsilyl)-7-azaindole-5-carboxylate

: 1310731-57-7
C₂₅H₃₁N₃O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

2: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

3: butan-1-ol / 16 h / 110 °C

4: diisobutylaluminium hydride / toluene / 2 h / -78 - 20 °C

5: manganese(IV) oxide / chloroform / 16 h / 20 °C

6: potassium tert-butylate / tetrahydrofuran / 16 h / 0 - 20 °C

7: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1.5 h / 20 °C

With manganese(IV) oxide; palladium 10% on activated carbon; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide; toluene; butan-1-ol; 6: |Wittig Olefination;
DOI:10.1016/j.bmcl.2012.11.108

Reference yield:

: 651744-48-8
4-chloro-1-triisopropylsilanyl-1H-pyrrolo[2,3-b]pyridine

: 1310731-57-7
C₂₅H₃₁N₃O₄S

Guidance literature:: Multi-step reaction with 8 steps

1: sec.-butyllithium / tetrahydrofuran / 0.67 h / -78 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

3: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

4: butan-1-ol / 16 h / 110 °C

5: diisobutylaluminium hydride / toluene / 2 h / -78 - 20 °C

6: manganese(IV) oxide / chloroform / 16 h / 20 °C

7: potassium tert-butylate / tetrahydrofuran / 16 h / 0 - 20 °C

8: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1.5 h / 20 °C

With manganese(IV) oxide; palladium 10% on activated carbon; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide; toluene; butan-1-ol; 7: |Wittig Olefination;
DOI:10.1016/j.bmcl.2012.11.108