3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1418012-35-7
• Molecular Formula: C₃₅H₃₇BF₂N₄O₄
• Molecular Weight: 626.511
• Mol file: 1418012-35-7.mol

Synonyms:3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-(2-acetoxyethen-1-yl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-33-5) + dimethyl amine (124-40-3) → 3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-35-7)

Guidance literature:

With water; In acetonitrile; for 1h;

DOI:10.1039/c2ob27004h

Reference yield:

C32H29BF2N2O6 (1206782-13-9) → 3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-35-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic anhydride / o-xylene / 0.02 h / Reflux

2: water / acetonitrile / 1 h

With water; acetic anhydride; In o-xylene; acetonitrile;

DOI:10.1039/c2ob27004h

Reference yield:

3,5-bis(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-35-7) → C37H37BF2N4O2 (1418012-44-8)

Guidance literature:

Multi-step reaction with 3 steps

1: water; trifluoroacetic acid / 0.02 h / Reflux

2: N,N-dimethyl-formamide / 0.02 h / Reflux

3: ethanol / 0.75 h / Reflux

With water; N,N-dimethyl-formamide; trifluoroacetic acid; In ethanol;

DOI:10.1039/c2ob27004h

upstream raw materials:

C₃₂H₂₉BF₂N₂O₆

3-(2-acetoxyethen-1-yl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

dimethyl amine

Downstream raw materials:

3,5-bis(2-formylmethyl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3,5-bis(2-acetoxyethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3,5-bis(2-chloroethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene