(2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

Base Information

Chemical Name:(2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol
CAS No.:96158-82-6
Molecular Formula:C₁₃H₁₈O₆S
Molecular Weight:302.348
Hs Code.:

Synonyms:(2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

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Technology Process of (2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

There total 10 articles about (2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 22566-82-1,23558-19-2,49858-49-3,63073-99-4,135891-42-8,7534-35-2
1-thio-β-D-glucopyranose

: 696-62-8
para-iodoanisole

: 96158-82-6
(2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: With pyridine; [nickel(II)dichloride(dimethoxyethane)]; zinc; In methanol; at 20 ℃; for 2h; Reagent/catalyst; Solvent; Time;
DOI:10.1002/chem.201302999

Reference yield:

: 85951-15-1
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 96158-82-6
(2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: With methanol; barium methoxide;
DOI:10.1021/jo01173a015

Reference yield:

: 2280-44-6
D-Glucose

: 696-63-9
4-Methoxybenzenethiol

: (2R,3S,4S,5R,6R)-2-(hydroxymethyl)-6-((4-methoxyphenyl)thio)tetrahydro-2H-pyran-3,4,5-triol

: 96158-82-6
(2R,3S,4S,5R,6S)-2-(hydroxymethyl)-6-[(4-methoxyphenyl)thio]tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: With 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine; In water; acetonitrile; at 0 ℃; for 1h; optical yield given as %de;
DOI:10.1246/cl.2009.458