Naphthalene, 1-methoxy-2-methyl- (6CI,7CI,8CI,9CI)

Base Information

• Chemical Name: Naphthalene, 1-methoxy-2-methyl- (6CI,7CI,8CI,9CI)
• CAS No.: 14093-86-8
• Molecular Formula: C12H12 O
• Molecular Weight: 172.227
• Mol file: 14093-86-8.mol

Synonyms:1-Methoxy-2-methylnaphthalene

Chemical Property of Naphthalene, 1-methoxy-2-methyl- (6CI,7CI,8CI,9CI)

Chemical Property:

• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

≥97% ^*data from raw suppliers

1-Methoxy-2-methylnaphthalene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Naphthalene, 1-methoxy-2-methyl- (6CI,7CI,8CI,9CI)

There total 6 articles about Naphthalene, 1-methoxy-2-methyl- (6CI,7CI,8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

methyl hypofluorite (36336-08-0) + 2-Methylnaphthalene (91-57-6,34468-07-0) → 1-methoxy-2-methylnaphthalene (14093-86-8)

Guidance literature:

In dichloromethane; acetonitrile; -45 deg C to room temperature;

DOI:10.1021/jo00058a052

Reference yield:

α-naphthol (90-15-3) + dimethyl sulfate (77-78-1) → 2-methylnaphthalen-1-ol (7469-77-4) + 1-methoxy-2-methylnaphthalene (14093-86-8) + 1-Methoxynaphthalene (2216-69-5)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) benzene, hexane, reflux, 2.) 3 h reflux;

Reference yield:

1-Methoxynaphthalene (2216-69-5) + methyl iodide (74-88-4) → 1-methoxy-2-methylnaphthalene (14093-86-8) + 8-methyl-1-methoxynaphthalene (60023-09-8)

Guidance literature:

1-Methoxynaphthalene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; cyclohexane; at 20 ℃; for 14h;

methyl iodide; In hexane; cyclohexane; at 20 ℃; for 2h; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/ja010456w

upstream raw materials:

2-methylnaphthalen-1-ol

dimethyl sulfate

α-naphthol

methyl hypofluorite

Downstream raw materials:

menadione

1-Acetoxy-4-benzyl-2-methyl-naphthalin

4-Benzyl-1-methoxy-2-methylnaphthalin

4-Benzyl-2-methyl-1-naphthol

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