tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

Base Information

Chemical Name:tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate
CAS No.:912275-37-7
Molecular Formula:C₂₃H₂₅F₆NO₃
Molecular Weight:477.447
Hs Code.:

Synonyms:tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

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Chemical Property of tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

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Technology Process of tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

There total 1 articles about tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 912275-35-5
4-(3,5-bis(trifluoromethyl)benzyloxy)-3-phenylbutanoic acid

: 75-65-0
tert-butyl alcohol

: 912275-37-7
tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

Guidance literature:: 4-(3,5-bis(trifluoromethyl)benzyloxy)-3-phenylbutanoic acid; With diphenyl phosphoryl azide; triethylamine; In toluene; for 1h; Heating / reflux;

tert-butyl alcohol; In toluene; for 20h; Heating / reflux;

Reference yield: 100.0%

: 912275-37-7
tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

: 912275-39-9
3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropylamine hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 1h;

Reference yield: 82.0%

: 912275-37-7
tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate

: 74-88-4
methyl iodide

: 912275-41-3
[3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]methylcarbamic acid tert-butyl ester

Guidance literature:: tert-butyl [3-(3,5-bis(trifluoromethyl)benzyloxy)-2-phenylpropyl]carbamate; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 20h;