Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester

Base Information

• Chemical Name: Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester
• CAS No.: 136298-22-1
• Molecular Formula: C₁₅H₁₈O₅
• Molecular Weight: 278.305

Synonyms:Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester

Chemical Property of Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester

Chemical Property:

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Technology Process of Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester

There total 3 articles about Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-deoxy-4,5-O-isopropylidene-3-O-benzoyl-D-threo-pentose diethyl dithioacetal (136298-20-9) → Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester (136298-22-1)

Guidance literature:

With boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; water;

DOI:10.1080/00397919108021033

Reference yield:

2-deoxy-4,5-O-isopropylidene-D-threo-pentose diethyl dithioacetal (67320-20-1) → Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester (136298-22-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / pyridine / 6 h / Ambient temperature

2: 90 percent / mercury(II) oxide, boron trifluoride etherate / tetrahydrofuran; H₂O

With pyridine; boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; water;

DOI:10.1080/00397919108021033

Reference yield:

benzoyl chloride (98-88-4) → Benzoic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-oxo-propyl ester (136298-22-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / pyridine / 6 h / Ambient temperature

2: 90 percent / mercury(II) oxide, boron trifluoride etherate / tetrahydrofuran; H₂O

With pyridine; boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; water;

DOI:10.1080/00397919108021033

upstream raw materials:

2-deoxy-4,5-O-isopropylidene-3-O-benzoyl-D-threo-pentose diethyl dithioacetal

2-deoxy-4,5-O-isopropylidene-D-threo-pentose diethyl dithioacetal

benzoyl chloride

Downstream raw materials:

2(R),3(R) 1,2-O-isopropylidene-3-O-benzoyl-5Z-undecene

(2R,4Z)-2-Benzoyloxydec-4-en-1-al

10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

Benzoic acid (Z)-(R)-1-((R)-1,2-dihydroxy-ethyl)-non-3-enyl ester

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