10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

Base Information

Chemical Name:10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate
CAS No.:136298-21-0
Molecular Formula:C₂₆H₃₈O₄
Molecular Weight:414.585
Hs Code.:

Synonyms:

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Chemical Property of 10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

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Technology Process of 10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

There total 10 articles about 10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60106-53-8
n-hexyltriphenylphosphonium iodide

: 136298-21-0
10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaNH₂, HMPA / 1.) THF, -78 deg C, 2.) THF, RT, 8 h

2: 95 percent / trifluoroacetic acid / H₂O / 0.5 h / 0 °C

3: 90 percent / Pb(OAc)4, NaHCO₃ / CH₂Cl₂ / 0.5 h / 0 °C

4: 1.) HMPA, n-BuLi / 1.) THF, -78 deg C, 2 h, 2.) THF, MeOH, -40 deg C, 4 h

5: diethyl ether

With lead(IV) acetate; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium hydrogencarbonate; sodium amide; trifluoroacetic acid; In diethyl ether; dichloromethane; water;
DOI:10.1080/00397919108021033

Reference yield:

: 111037-24-2
Benzoic acid (Z)-(R)-1-((R)-1,2-dihydroxy-ethyl)-non-3-enyl ester

: 136298-21-0
10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Pb(OAc)4, NaHCO₃ / CH₂Cl₂ / 0.5 h / 0 °C

2: 1.) HMPA, n-BuLi / 1.) THF, -78 deg C, 2 h, 2.) THF, MeOH, -40 deg C, 4 h

3: diethyl ether

With lead(IV) acetate; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium hydrogencarbonate; In diethyl ether; dichloromethane;
DOI:10.1080/00397919108021033

Reference yield:

: 111037-23-1
2(R),3(R) 1,2-O-isopropylidene-3-O-benzoyl-5Z-undecene

: 136298-21-0
10(R)-methyl-10-O-benzoyl-8E,12Z-octadecadienoate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / trifluoroacetic acid / H₂O / 0.5 h / 0 °C

2: 90 percent / Pb(OAc)4, NaHCO₃ / CH₂Cl₂ / 0.5 h / 0 °C

3: 1.) HMPA, n-BuLi / 1.) THF, -78 deg C, 2 h, 2.) THF, MeOH, -40 deg C, 4 h

4: diethyl ether

With lead(IV) acetate; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium hydrogencarbonate; trifluoroacetic acid; In diethyl ether; dichloromethane; water;
DOI:10.1080/00397919108021033