1-phenoxygermatrane

Base Information

Chemical Name:1-phenoxygermatrane
CAS No.:76228-30-3
Molecular Formula:C₁₂H₁₇GeNO₄
Molecular Weight:311.861
Hs Code.:

Synonyms:1-phenoxygermatrane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenoxygermatrane

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Technology Process of 1-phenoxygermatrane

There total 3 articles about 1-phenoxygermatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 102-71-6,64114-46-1
triethanolamine

: tetramethoxygermanium

: 76228-30-3
1-phenoxygermatrane

Guidance literature:: With phenol; In xylene; boiled for 3 h;

Reference yield: 67.0%

: 20836-42-4
2,2',2''-tris(trimethylsiloxy)triethylamine

: tetramethoxygermanium

: 76228-30-3
1-phenoxygermatrane

Guidance literature:: With phenol; In xylene; byproducts: (CH3)3Si(CH3O); boiled for 3 h; elem. anal.;

Reference yield: 21.0%

: 67453-19-4
germatrane

: 76228-30-3
1-phenoxygermatrane

: 1333-74-0
hydrogen

Guidance literature:: With phenol; In o-xylene=o-xylol; under dry N2; a flask with thermometer and reflux condenser charged with germatrane, phenol, sodium phenoxide (boiling in o-xylene); boiled for3.5 h; mixt. (44% of phenoxygermatrane) isolated from soln., detected by PMR;