N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

Base Information

Chemical Name:N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal
CAS No.:117559-87-2
Molecular Formula:C₂₀H₂₇NO₃Si
Molecular Weight:357.525
Hs Code.:

Synonyms:N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

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Technology Process of N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

There total 4 articles about N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-30-8
4-amino-phenol

: 117559-87-2
N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / tetrahydrofuran / 0.5 h

2: triethylamine / tetrahydrofuran / 1 h / 1.) 0.5 h, 2.) in THF, 1 h

3: LiClO₄ / 2.75 h / 6 °C / anodic oxidation: Pt electrode, 0.1 A

With 1H-imidazole; lithium perchlorate; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00262a018

Reference yield:

: 111359-74-1
4-[(tert-butyldimethylsilyl)oxy]aniline

: 117559-87-2
N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 1.) 0.5 h, 2.) in THF, 1 h

2: LiClO₄ / 2.75 h / 6 °C / anodic oxidation: Pt electrode, 0.1 A

With lithium perchlorate; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00262a018

Reference yield:

: 98-88-4
benzoyl chloride

: 117559-87-2
N-benzoylbenzoquinone imine methyl tert-butyldimethylsilyl ketal

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 1.) 0.5 h, 2.) in THF, 1 h

2: LiClO₄ / 2.75 h / 6 °C / anodic oxidation: Pt electrode, 0.1 A

With lithium perchlorate; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00262a018