2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

Base Information

Chemical Name:2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate
CAS No.:187960-21-0
Molecular Formula:C₂₀H₂₂N₄O₈
Molecular Weight:446.417
Hs Code.:

Synonyms:2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

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Chemical Property of 2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

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Technology Process of 2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

There total 1 articles about 2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 117541-83-0
2,5-bis-(2-acetoxyethyloxy)aniline

: 100-01-6,104810-17-5
4-nitro-aniline

: 187960-21-0
2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

Guidance literature:: 4-nitro-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃; pH=< 1;

2,5-bis-(2-acetoxyethyloxy)aniline; In water; acetone; at 20 ℃;

Reference yield: 81.0%

: 57154-24-2
3-methyl-N,N-dioctylaniline

: 187960-21-0
2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

: 1439365-36-2
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl)diacetate

Guidance literature:: 2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate; With nitrosylsulfuric acid; In 1-methyl-pyrrolidin-2-one; at 5 - 40 ℃; for 1.5h;

3-methyl-N,N-dioctylaniline; In 1-methyl-pyrrolidin-2-one; water; acetone; at 20 ℃; Cooling with ice;

Reference yield:

: 187960-21-0
2,2'-(2-amino-5-((4-nitrophenyl)diazenyl)-1 ,4-phenylene)bis(oxy)bis(ethane-2, 1-diyl) diacetate

: 1439365-37-3
2,2'-(2-((4-(dioctylamino)-2-methylphenyl)diazenyl)-5-((4-n itrophenyl)diazenyl)-1 ,4-phenylene )bis( oxy)diethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 1.5 h / 5 - 40 °C

1.2: 20 °C / Cooling with ice

2.1: lithium hydroxide / tetrahydrofuran / 20 °C

With nitrosylsulfuric acid; lithium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;