N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide

Base Information

• Chemical Name: N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide
• CAS No.: 1374016-15-5
• Molecular Formula: C₂₃H₂₃NO₄S₂
• Molecular Weight: 441.572
• Mol file: 1374016-15-5.mol

Synonyms:N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide

Chemical Property of N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide

There total 9 articles about N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

di(4-tosyl)amine (3695-00-9) + isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) → N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide (1374016-15-5)

Guidance literature:

With ((4-methyl-N-tosylphenyl)sulfonamido)(phenyl)-λ³-iodanyl acetate; In dichloromethane; at 25 ℃; for 20h;

DOI:10.1021/ja3013193

Reference yield: 87.0%

acetoxy((4-methyl)-N-tosylbenzenesulfonamidyl)iodosobenzene (1345824-06-7) + di(4-tosyl)amine (3695-00-9) + isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) → N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide (1374016-15-5)

Guidance literature:

In dichloromethane; at 25 ℃; for 20h;

Reference yield: 79.0%

3-phenylbut-3-enoic acid (5155-87-3) + bis[(4-methyl)-N-tosylbenzenesulfonamidyl]iodosobenzene (1414869-25-2) → N-[2-(phenyl)prop-2-en-1-yl]-N,N-bis(p-toluenesulfonyl)imide (1374016-15-5)

Guidance literature:

bis[(4-methyl)-N-tosylbenzenesulfonamidyl]iodosobenzene; With [bis(acetoxy)iodo]benzene; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h; Inert atmosphere;

3-phenylbut-3-enoic acid; In 1,2-dichloro-ethane; at 80 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ol5022433

upstream raw materials:

(2,2-dideuterio-1-methyl-vinyl)-benzene

di(4-tosyl)amine

isopropenylbenzene

α-methylstyrene-methyl-d₃

Downstream raw materials:

N-[2-(phenyl)prop-2-en-1-yl]-N-(p-toluenesulfonyl)amide