Tetrabromomolybdenum

Base Information

Chemical Name:Tetrabromomolybdenum
CAS No.:13520-59-7
Molecular Formula:Br4Mo
Molecular Weight:415.556
Hs Code.:
DSSTox Substance ID:DTXSID00448625
Wikipedia:Molybdenum(IV)_bromide
Wikidata:Q4096884
Mol file:13520-59-7.mol

Synonyms:Tetrabromomolybdenum;MOLYBDENUM TETRABROMIDE;13520-59-7;DTXSID00448625

Suppliers and Price of Tetrabromomolybdenum

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Tetrabromomolybdenum

Chemical Property:

Melting Point:decomposes [KIR81]
PSA：0.00000
LogP:-11.98400
Water Solubility.:reacts with H2O [LID94]
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:417.57466
Heavy Atom Count:5
Complexity:19.1

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:Br[Mo](Br)(Br)Br

Technology Process of Tetrabromomolybdenum

There total 2 articles about Tetrabromomolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 7726-95-6
bromine

: 7439-98-7
molybdenum

: 13446-57-6
molybdenum(III) bromide

: 13520-59-7
molybdenum tetrabromide

Guidance literature:: In neat (no solvent); passing dry CO2 satd. with bromine vapor over Mo at 350-400°C;; washing with cold HBr containing water;;

Reference yield:

: 7726-95-6
bromine

: 7439-98-7
molybdenum

: 13446-57-6
molybdenum(III) bromide

: molybdenum dioxydibromide

: 13520-59-7
molybdenum tetrabromide

Guidance literature:: In neat (no solvent); passing Br2 vapor over moderately heated Mo;; no analysis;;

Reference yield: 71.0%

: 13520-59-7
molybdenum tetrabromide

: 1779-49-3
Methyltriphenylphosphonium bromide

: 74-95-3
1,1-dibromomethane

: 2(P(C₆H₅)3CH₃)⁽¹⁺⁾*{MoBr₆}^(2-)*2CH₂Br₂

Guidance literature:: In further solvent(s); exclusion of moisture; 4.13 g MoBr4 and 7.10 g (PPh3Me)Br in CH2Br2 stirred at room temp. for 12 h and subsequently heated for 3 h under reflux; after cooling to -20°C the black crystalline ppt. is filtered off, washed with CH2Br2, and dried in vac.; elem. anal.;