tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane

Base Information

Chemical Name:tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane
CAS No.:74559-40-3
Molecular Formula:C₄H₁₀O₂*C₃₆H₉₉NdSi₉Sn₃
Molecular Weight:1375.44
Hs Code.:

Synonyms:tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane

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Chemical Property of tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane

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Technology Process of tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane

There total 1 articles about tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.2%

: 34501-61-6
Tris<(trimethylsilyl)-methyl>stannan

: neodymium(III) hexamethyldisilazide

: 74559-40-3
tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

Guidance literature:: In 1,2-dimethoxyethane; (vac.) to soln. of Nd compd. was added tin compd. and mixt. was heated at 100°C for 15 h; solvent was removed in vac., residue washed with hexane and dried in vac.; elem. anal.; (Me3Si)2NH was detected by GLC anal. of volatiles;
DOI:10.1016/S0022-328X(00)85913-6

Reference yield: 95.7%

: 74559-40-3
tris[tris(trimethylsilylmethyl)stannyl]neodymium*1,2-dimethoxyethane

: 94-36-0
dibenzoyl peroxide

: ((CH₃)3SiCH₂)3SnNd(OCOC₆H₅)2

: 42202-20-0
((CH₃)3SiCH₂)3Sn(OCOC₆H₅)

Guidance literature:: In benzene; soln. of Nd-Sn complex was shaken with soln. of benzoylperoxide at 50°C for 12 h; Sn-Nd complex pptd.; elem. anal.; org. layer was sepd. by distn.;
DOI:10.1016/S0022-328X(00)85913-6