Technology Process of C38H46O7S
There total 4 articles about C38H46O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
at 0 ℃;
for 23h;
Inert atmosphere;
DOI:10.1039/c003464a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diisobutylaluminium hydride / toluene / 4 h / -78 °C
2: potassium hexacyanoferrate(III); methanesulfonamide; potassium osmate(VI); (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane] / tert-butyl alcohol; water / 72 h / 0 °C
3: triethylamine / dichloromethane / 15 h / 20 °C
With
potassium osmate(VI); methanesulfonamide; diisobutylaluminium hydride; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; triethylamine; potassium hexacyanoferrate(III);
In
dichloromethane; water; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / dichloromethane / 20 h / 20 °C
2: diisobutylaluminium hydride / toluene / 4 h / -78 °C
3: potassium hexacyanoferrate(III); methanesulfonamide; potassium osmate(VI); (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane] / tert-butyl alcohol; water / 72 h / 0 °C
4: triethylamine / dichloromethane / 15 h / 20 °C
With
potassium osmate(VI); methanesulfonamide; diisobutylaluminium hydride; potassium carbonate; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; triethylamine; potassium hexacyanoferrate(III);
In
dichloromethane; water; toluene; tert-butyl alcohol;