1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

Base Information

Chemical Name:1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane
CAS No.:137070-56-5
Molecular Formula:C₃₀H₂₆Cl₂O₃
Molecular Weight:505.441
Hs Code.:

Synonyms:1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

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Technology Process of 1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

There total 5 articles about 1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 67-66-3,8013-54-5
chloroform

: 131544-81-5,131544-82-6
1-<4-(benzyloxy)phenyl>-1,2-bis(4-methoxyphenyl)ethene

: 137070-56-5,131544-83-7
1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; for 30h;
DOI:10.1021/jm00106a052

Reference yield:

: 1-(4-Benzyloxyphenyl)-1,2-bis(4-methoxyphenyl)ethene

: C₆ H₆ -petroleum ether

: 60-29-7,927820-24-4
diethyl ether

: 75-09-2
dichloromethane

: 7732-18-5
water

: 137070-56-5,131544-83-7
1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In C₆ H₆; chloroform; Petroleum ether;

Reference yield:

: 6793-92-6
p-benzyloxyphenylbromide

: 137070-56-5,131544-83-7
1,1-dichloro-2-<4-(benzyloxy)phenyl>-2,3-bis(4-methoxyphenyl)cyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, I₂, EtBr₂ / 1.) THF, reflux, 2 h, 2.) THF, reflux, 18 h

2: 2N H₂SO₄ / H₂O

3: 26 percent / benzyltriethylammonium chloride, 50percent aq. NaOH / 30 h

With sodium hydroxide; sulfuric acid; N-benzyl-N,N,N-triethylammonium chloride; iodine; magnesium; In water;
DOI:10.1021/jm00106a052