BENZYL ALCOHOL, [7-14C]

Base Information

• Chemical Name: BENZYL ALCOHOL, [7-14C]
• CAS No.: 13057-53-9
• Molecular Formula: C7H8 O
• Molecular Weight: 110.129
• Mol file: 13057-53-9.mol

Synonyms:Benzyl-a-14C alcohol (6CI,7CI,8CI)

Chemical Property of BENZYL ALCOHOL, [7-14C]

Chemical Property:

• PSA: 20.23000
• LogP: 1.17890
• Storage Temp.: 2-8°C

Purity/Quality:

BENZYL ALCOHOL[7-14C] 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: R

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL ALCOHOL, [7-14C]

There total 3 articles about BENZYL ALCOHOL, [7-14C] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

[carbonyl-(14)C]benzoic acid (1589-66-8) → [1-14C]benzyl alcohol (13057-53-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 15h;

DOI:10.1002/1099-1344(20001015)43:11<1119::AID-JLCR398>3.0.CO;2-D

Reference yield:

[carboxyl-14C]-methyl benzoate (18615-08-2) → [1-14C]benzyl alcohol (13057-53-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/(SICI)1099-1344(1998110)41:11<977::AID-JLCR143>3.0.CO;2-J

Reference yield:

→ [1-14C]benzyl alcohol (13057-53-9)

Guidance literature:

DOI:10.1002/jlcr.2590090318 DOI:10.1002/jlcr.2590090112 DOI:10.1002/jlcr.2590070111 DOI:10.1002/jlcr.2580120106 DOI:10.1002/jlcr.2590060310

upstream raw materials:

[carbonyl-(14)C]benzoic acid

[carboxyl-14C]-methyl benzoate

Downstream raw materials:

[carbonyl‐¹⁴C] benzaldehyde

C₁₀⁽¹⁴⁾CH₁₃BrO₂

4-[1-methyl-2,4-dioxo-6-(3-phenylprop-1-yn-1-yl)-1,4-dihydro-2H-quinazolin-3-ylmethyl]benzoic acid

4-[1-methyl-2,4-dioxo-6-(3-phenyl-[3-¹⁴C]prop-1-ynyl)-1,4-dihydro-2Hquinazolin-3-ylmethyl]benzoic acid

Refernces

• 1、 Koltai,Alexin,Rutkai,Toth-Sarudy. "Synthesis of optically pure (D-phenyl[3-14C]alanine". . p. 977 - 982. Retrieved 1998.
• 2、 Le, Diem Duy,Zhang, Yinsheng,Chien, David H.,Moravek, Josef. "Syntheses of N-t-butyl-α-phenylnitrone-α-14C and α-(4-pyridyl-1-oxide)-N-t-butylnitrone-α-14C". . p. 1119 - 1125. Retrieved 2007/10/03.