methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate

Base Information

• Chemical Name: methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate
• CAS No.: 161038-45-5
• Molecular Formula: C₁₉H₁₉N₃O₅
• Molecular Weight: 369.377

Synonyms:methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate

Chemical Property of methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate

Chemical Property:

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Technology Process of methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate

There total 4 articles about methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methanol (67-56-1) + N-<1-<(azidocarbonyl)methyl>-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide (161038-47-7) → methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate (161038-45-5)

Guidance literature:

With triethylamine; for 48h; Ambient temperature;

DOI:10.1002/jhet.5570310601

Reference yield: 54.0%

methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate (161038-38-6) → methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate (161038-45-5)

Guidance literature:

With sodium azide; sulfuric acid; In chloroform; at 0 - 20 ℃; for 2.33333h;

DOI:10.1002/jhet.5570310601

Reference yield: 28.0%

methanol (67-56-1) + N-<1-<(azidocarbonyl)methyl>-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide (161038-47-7) → methyl <<3-(benzoylamino)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>methyl>carbamate + methyl 3-(benzoylamino)-2,5,6,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetate (161038-45-5)

Guidance literature:

for 2h; Ambient temperature;

DOI:10.1002/jhet.5570310601

upstream raw materials:

methanol

N-<1-<(azidocarbonyl)methyl>-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

Downstream raw materials:

N-<1-(carbazoylmethyl)-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

N-<1-<(azidocarbonyl)methyl>-2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

N-<2,5,6,7,8,9-hexahydro-1-(isocyanatomethyl)-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

N-<2,5,6,7,8,9-hexahydro-2,5-dioxo-1H-pyrido<3,2-c>azepin-3-yl>benzamide

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