(E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide
• CAS No.: 1228679-43-3
• Molecular Formula: C₁₆H₁₈N₂O₃S
• Molecular Weight: 318.397
• Mol file: 1228679-43-3.mol

Synonyms:(E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Chemical Property of (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide

There total 3 articles about (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

toluene-4-sulfonic acid hydrazide (1576-35-8) + 1-(4-methoxyphenyl)ethanone (100-06-1) → (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1228679-43-3)

Guidance literature:

In hexane; at 20 ℃;

DOI:10.1021/acs.orglett.5b00398

Reference yield: 90.0%

toluene-4-sulfonic acid hydrazide (1576-35-8) + 4-methoxyphenylacetylen (768-60-5) → (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1228679-43-3)

Guidance literature:

With [(THD-Dipp)AuOTf]; In neat (no solvent); at 100 ℃; regioselective reaction; Catalytic behavior; Green chemistry;

DOI:10.1002/adsc.201500658

Reference yield:

toluene-4-sulfonic acid hydrazide (1576-35-8) + 1-(4-methoxyphenyl)ethanone (100-06-1) → (E)-N′-(1-(4-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1228679-43-3) + (Z)-4-methoxyacetophenone tosylhydrazone

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 3h;

DOI:10.1021/ol300652k

upstream raw materials:

toluene-4-sulfonic acid hydrazide

1-(4-methoxyphenyl)ethanone

4-methoxyphenylacetylen

Downstream raw materials:

1-(1-(4-methoxyphenyl)vinyl)-3-methylbenzene

1-methoxy-4-[1-(4-methylphenyl)vinyl]benzene

1-chloro-3-(1-(4-methoxyphenyl)vinyl)benzene

1,1-bis-(4-methoxyphenyl)ethylene