(FC₆H₄CHCH₂)(CO)4Fe

Base Information

• Chemical Name: (FC₆H₄CHCH₂)(CO)4Fe
• CAS No.: 83721-74-8
• Molecular Formula: C₁₂H₇FFeO₄
• Molecular Weight: 290.031
• Mol file: 83721-74-8.mol

Synonyms:(FC₆H₄CHCH₂)(CO)4Fe

Chemical Property of (FC₆H₄CHCH₂)(CO)4Fe

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of (FC₆H₄CHCH₂)(CO)4Fe

There total 1 articles about (FC₆H₄CHCH₂)(CO)4Fe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

diiron nonacarbonyl (15321-51-4) + para-fluorostyrene (405-99-2) → iron pentacarbonyl (13463-40-6,37220-42-1) + triiron dodecarbonyl (17685-52-8) + (FC6H4CHCH2)(CO)4Fe (83721-74-8)

Guidance literature:

In pentane; under Ar, equimolar amts. of FcolC6H4CHCH2 and Fe2(CO)9 stirred in pentane at 20°C for 2-3 d; filtered, evapd. at 20°C/1 Torr, chromd. (neutral Al2O3 (activity I), pentane, at 5°C), concd., admixture sepd. by short-path distn. (20°C; 0.001 Torr), crystals purified by crystn. from pentaneat -80°C; elem. anal.;

DOI:10.1016/S0022-328X(00)85703-4

Reference yield:

(FC6H4CHCH2)(CO)4Fe (83721-74-8) → triiron dodecarbonyl (17685-52-8)

Guidance literature:

In not given; decompn. in soln. or in melt;

DOI:10.1016/S0022-328X(00)85703-4

upstream raw materials:

diiron nonacarbonyl

para-fluorostyrene

Downstream raw materials:

triiron dodecarbonyl