(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

Base Information

Chemical Name:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane
CAS No.:162088-71-3
Molecular Formula:C₄₂H₈₂BrClGeSi₆
Molecular Weight:943.573
Hs Code.:

Synonyms:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

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Chemical Property of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

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Technology Process of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

There total 1 articles about (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 10038-98-9
germaniumtetrachloride

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 162088-71-3
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

Guidance literature:: With t-BuLi; NH₄Cl; In tetrahydrofuran; pentane; Ar-atmosphere; stirring (-78°C, 10 min), GeCl4 addn. (-78°C), Grignard reagent addn. (room temp.), stirring (refluxing, 10 h), NH4Cl soln. (aq) addn.; concg. (reduced pressure), CHCl3 and HCl addn., extg. (CHCl3), drying (MgSO4), evapn. (reduced pressure), repptn. (CH2Cl2 / EtOH, room temp.); elem. anal.;
DOI:10.1021/om00002a055

Reference yield: 99.0%

: 16853-85-3
lithium aluminium tetrahydride

: 162088-71-3
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

: 162088-73-5
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

Guidance literature:: With NH₄Cl; In tetrahydrofuran; water; Ar-atmosphere; refluxing (10 h), NH4Cl soln. (aq) addn.; washing (HCl soln.), extg. (CHCl3), drying (MgSO4), evapn. (reduced pressure), repptn. (CH2Cl2 / EtOH, room temp.); elem. anal.;
DOI:10.1021/om00002a055

Reference yield: 81.0%

: 10544-50-0
sulfur

: 162088-71-3
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

: 152291-64-0
5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

Guidance literature:: With t-BuLi; In 1,2-dimethoxyethane; pentane; Ar-atmosphere; stirring (-78°C, 5 min), S8 addn., refluxing (10 h); evapn. (reduced pressure), recrystn. (CHCl3), chromy. (SiO2, hexane), recrystn. (EtOH); elem. anal.;
DOI:10.1021/om00002a055