2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

Base Information

Chemical Name:2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide
CAS No.:1589599-11-0
Molecular Formula:C₁₉H₂₅N₃O₆S
Molecular Weight:423.49
Hs Code.:

Synonyms:2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

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Chemical Property of 2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

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Technology Process of 2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

There total 5 articles about 2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18226-11-4
N-(2-hydroxy-ethyl)-2-nitro-benzenesulfonamide

: 1589598-96-8
3-[(4-methoxyphenyl)methyl]-1,2,3-oxathiazinane-2,2-dione

: 1589599-11-0
2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

Guidance literature:: N-(2-hydroxy-ethyl)-2-nitro-benzenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;

3-[(4-methoxyphenyl)methyl]-1,2,3-oxathiazinane-2,2-dione; In N,N-dimethyl-formamide; at 80 ℃; for 24h;
DOI:10.1039/c3ob42512f

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1589599-11-0
2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / dichloromethane; water / 24 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

2.2: 24 h / 80 °C

With sodium hydride; sodium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42512f

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1589599-11-0
2-hydroxy-N-(3'-{[(4-methoxyphenyl)methyl]amino}propyl)-N-(2'-nitrophenyl)ethane-1-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium cyanoborohydride / methanol / 16 h / 20 °C

2.1: thionyl chloride; triethylamine; 1H-imidazole / dichloromethane / 3 h / -60 °C

3.1: ruthenium(III) chloride trihydrate; sodium periodate / acetonitrile; water / 0 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

4.2: 24 h / 80 °C

With 1H-imidazole; sodium periodate; thionyl chloride; ruthenium(III) chloride trihydrate; sodium hydride; sodium cyanoborohydride; triethylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3ob42512f