C₂₈H₂₂ClF₉N₂O₃

Base Information

Chemical Name:C₂₈H₂₂ClF₉N₂O₃
CAS No.:1254313-02-4
Molecular Formula:C₂₈H₂₂ClF₉N₂O₃
Molecular Weight:640.933
Hs Code.:

C<sub>28</sub>H<sub>22</sub>ClF<sub>9</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₈H₂₂ClF₉N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₂ClF₉N₂O₃

Chemical Property:

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Technology Process of C₂₈H₂₂ClF₉N₂O₃

There total 7 articles about C₂₈H₂₂ClF₉N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254318-25-6
3-amino-N-[2-ethyl-4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)-6-methylphenyl]-2-methoxy benzamide

: 118-91-2
ortho-chlorobenzoic acid

: 1254313-02-4
C₂₈H₂₂ClF₉N₂O₃

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In ISOPROPYLAMIDE; at 100 ℃; for 16h;

Reference yield:

: 573-54-6
2-bromo-3-nitro-benzoic acid

: 1254313-02-4
C₂₈H₂₂ClF₉N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 1 h / 100 °C

2.1: pyridine / tetrahydrofuran / 18 h / 20 °C / Reflux

2.2: 41 h / 20 °C

3.1: potassium carbonate / 16 h / 20 °C

4.1: hydrogenchloride; tin(ll) chloride / water; isopropyl alcohol / 0 - 80 °C

4.2: pH 7 - 8

5.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 100 °C

With pyridine; hydrogenchloride; thionyl chloride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; ISOPROPYLAMIDE; water; isopropyl alcohol; toluene;

Reference yield:

: 317-46-4
2-fluoro-3-nitro-benzoic acid

: 1254313-02-4
C₂₈H₂₂ClF₉N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Reflux

2.1: pyridine / tetrahydrofuran / 6 h / 20 °C / Reflux

3.1: potassium carbonate / 16 h / 20 °C

4.1: hydrogenchloride; tin(ll) chloride / water; isopropyl alcohol / 0 - 80 °C

4.2: pH 7 - 8

5.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 100 °C

With pyridine; hydrogenchloride; oxalyl dichloride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; ISOPROPYLAMIDE; water; isopropyl alcohol;