[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane

Base Information

• Chemical Name: [2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane
• CAS No.: 1003010-59-0
• Molecular Formula: C₃₂H₂₆BF₁₀P
• Molecular Weight: 642.327
• Mol file: 1003010-59-0.mol

Synonyms:[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane

Chemical Property of [2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane

There total 1 articles about [2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

dimesitylvinylphosphine (1003010-54-5) + bis(pentafluorophenyl)borohydride (165612-94-2) → [2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane (1003010-59-0)

Guidance literature:

In pentane; at 20 ℃; for 1h;

DOI:10.1002/anie.200801432

Reference yield: 92.0%

[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane (1003010-59-0) + 1,1,1-trifluoro-4-phenylbut-3-yn-2-one (58518-08-4) → OC(CF3)C2(Ph)Mes2PCH2CH2B(C6F5)2

Guidance literature:

In pentane; room temp.;

DOI:10.1002/anie.201101051

Reference yield: 87.0%

[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane (1003010-59-0) → Mes2HPCH2CH2BCl(C6F5)2 (1403338-72-6)

Guidance literature:

With hydrogenchloride; In diethyl ether; benzene; Inert atmosphere;

DOI:10.1002/ejic.201200288

upstream raw materials:

dimesitylvinylphosphine

bis(pentafluorophenyl)borohydride

Downstream raw materials:

((CH₃)3C₆H₂)2PCH₂CH₂B(C₆F₅)2(C₅H₄C(CH₃)2C₅H₄C(CH₃)2)

(C₆H₂(CH₃)3)2PCH₂CH₂B(C₆F₅)2CCH₂CHC₅H₂(CH₃)2N(CH₃)2

[2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate

C₄₂H₃₄BF₁₀OP