[2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate

Base Information

• Chemical Name: [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate
• CAS No.: 1003010-56-7
• Molecular Formula: C₃₂H₂₈BF₁₀P
• Molecular Weight: 644.343
• Mol file: 1003010-56-7.mol

Synonyms:[2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate

Chemical Property of [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate

There total 8 articles about [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

Ph2P-C2H4-B(C6F5)2 (1003010-55-6) → [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate (1003010-56-7)

Guidance literature:

With hydrogen; In pentane; at 20 ℃; for 0.25h; under 1125.11 Torr;

DOI:10.1039/b710475h

Reference yield: 60.0%

Ph2P-C2H4-B(C6F5)2 (1003010-55-6) + hydrogen (1333-74-0) → [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate (1003010-56-7)

Guidance literature:

In pentane; High Pressure; Mes2PC2H4B(C6F5)2 in pentane stirred in H2 atm (1.5 bar) at room temp. for 15 min;

DOI:10.1039/b710475h

Reference yield: 55.0%

dimesitylvinylphosphine (1003010-54-5) + bis(pentafluorophenyl)borohydride (165612-94-2) → [2-(dimesitylphosphonio)ethyl]bis(pentafluorophenyl)hydridoborate (1003010-56-7)

Guidance literature:

dimesitylvinylphosphine; bis(pentafluorophenyl)borohydride; In pentane;

With hydrogen; In pentane; at 20 ℃; for 0.25h; under 1875.19 Torr;

DOI:10.1002/anie.200801432

upstream raw materials:

Ph₂P-C₂H₄-B(C₆F₅)2

hydrogen

dimesitylvinylphosphine

bis(pentafluorophenyl)borohydride

Downstream raw materials:

(Z)-4,4-dimethyl-1-phenylpent-1-en-3-one