1H-Benzimidazole,6-chloro-4-nitro-(9CI)

Base Information

• Chemical Name: 1H-Benzimidazole,6-chloro-4-nitro-(9CI)
• CAS No.: 10597-49-6
• Molecular Formula: C7H4 Cl N3 O2
• Molecular Weight: 197.57856
• Mol file: 10597-49-6.mol

Synonyms:1H-Benzimidazole,6-chloro-4-nitro- (9CI); Benzimidazole, 6-chloro-4-nitro- (6CI,7CI,8CI)

Chemical Property of 1H-Benzimidazole,6-chloro-4-nitro-(9CI)

Chemical Property:

• PSA: 74.50000
• LogP: 2.64770

Purity/Quality:

98%,99%, ^*data from raw suppliers

6-Chloro-4-nitro-1H-benzimidazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Benzimidazole,6-chloro-4-nitro-(9CI)

There total 1 articles about 1H-Benzimidazole,6-chloro-4-nitro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formic acid (64-18-6) + 5-chloro-3-nitro-o-phenylenediamine (42389-30-0) → 6-chloro-4-nitrobenzimidazole (10597-49-6)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/ja01621a043

Reference yield:

6-chloro-4-nitrobenzimidazole (10597-49-6) → N-(6-Chloro-1H-benzoimidazol-4-yl)-benzamide (82326-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Raney nickel / ethanol

2: 90 percent / pyridine / dimethylformamide / Ambient temperature

With pyridine; hydrogen; nickel; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00350a002

Reference yield:

6-chloro-4-nitrobenzimidazole (10597-49-6) → 6-chloro-1(3)H-benzimidazol-4-ylamine (10597-55-4)

Guidance literature:

With hydrogenchloride; tin(ll) chloride;

DOI:10.1021/ja01621a043

upstream raw materials:

formic acid

5-chloro-3-nitro-o-phenylenediamine

Downstream raw materials:

6-chloro-1⁽³⁾H-benzimidazol-4-ylamine

N-(6-Chloro-1H-benzoimidazol-4-yl)-benzamide

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