[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃

Base Information

• Chemical Name: [B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃
• CAS No.: 1334305-66-6
• Molecular Formula: CF₃O₃S*C₂₈H₃₃BN₃O
• Molecular Weight: 587.471

Synonyms:[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃

Chemical Property of [B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃

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Technology Process of [B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃

There total 4 articles about [B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B(OH)(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide (1334305-64-4) + methyl trifluoromethanesulfonate (333-27-7) → [B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3 (1334305-66-6)

Guidance literature:

In dichloromethane; Inert atmosphere;

DOI:10.1039/c1cc13089g

Reference yield:

2,4-dimethyl-1H-pyrrole (625-82-1) → [B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3 (1334305-66-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

1.2: 0.25 h / 20 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: dichloromethane / Inert atmosphere

With trifluoroacetic acid; In dichloromethane;

DOI:10.1039/c1cc13089g

Reference yield:

phenylborondichloride (873-51-8) → [B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)](1+)*O3SCF3(1-)=[B(OH)(C6H5)((CH3)3NC6H4C(C4H(CH3)2N)2)]O3SCF3 (1334305-66-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

1.2: 0.25 h / 20 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: dichloromethane / Inert atmosphere

With trifluoroacetic acid; In dichloromethane;

DOI:10.1039/c1cc13089g

upstream raw materials:

2,4-dimethyl-1H-pyrrole

10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

methyl trifluoromethanesulfonate

phenylborondichloride

Downstream raw materials:

[BF(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[BF(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃

[B⁽¹⁸⁾F(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]⁽¹⁺⁾*O₃SCF₃^(1-)=[B⁽¹⁸⁾F(C₆H₅)((CH₃)3NC₆H₄C(C₄H(CH₃)2N)2)]O₃SCF₃

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