(1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

Base Information

Chemical Name:(1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester
CAS No.:1444010-74-5
Molecular Formula:C₁₉H₂₃BClF₃O₂
Molecular Weight:386.65
Hs Code.:

Synonyms:(1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

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Chemical Property of (1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

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Technology Process of (1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

There total 3 articles about (1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-09-2
dichloromethane

: 1444010-73-4
(3-trifluoromethylbenzyl)boronic acid (+)-pinane-2,3-diyl diester

: 1444010-74-5
(1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

Guidance literature:: dichloromethane; With n-butyllithium; In tetrahydrofuran; at -100 ℃; for 0.583333h;

(3-trifluoromethylbenzyl)boronic acid (+)-pinane-2,3-diyl diester; With zinc(II) chloride; In tetrahydrofuran; hexane; at -100 - 20 ℃;

Reference yield:

: 1190235-39-2
4,4,5,5-tetramethyl-2-[[3-(trifluoromethyl)phenyl]methyl]-1,3,2-dioxaborolane

: 1444010-74-5
(1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 12 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.58 h / -100 °C

2.2: -100 - 20 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether;

Reference yield:

: 402-23-3
1-bromomethyl-3-trifluoromethylbenzene

: 1444010-74-5
(1S)-1-chloro-2-(3-trifluoromethylphenyl)-ethylboronic acid (+)-pinane-2,3-diyl diester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 12 h / 100 °C

2.1: diethyl ether / 12 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran / 0.58 h / -100 °C

3.2: -100 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; diethyl ether;