(10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone

Base Information

Chemical Name:(10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone
CAS No.:1642568-72-6
Molecular Formula:C₂₂H₁₆N₂O₃
Molecular Weight:356.381
Hs Code.:

Synonyms:(10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone

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Chemical Property of (10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone

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Technology Process of (10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone

There total 2 articles about (10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 930-88-1
N-methylmaleimide

: 5653-11-2
α-(1,2,3,4-Tetrahydro-2-isochinolyl)-acetophenon

: 1642568-72-6
(10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone

Guidance literature:: With N-hydroxyphthalimide; tetraethylammonium bromide; In methanol; at 25 ℃; for 12h; regioselective reaction; Electrochemical reaction; Green chemistry;
DOI:10.1039/c9cc04336e

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 532-27-4,108321-66-0,164322-25-2
1-chloroacetophenone

: 1642568-72-6
(10-methyl-9,11-dioxo-6,9,10,11-tetrahydro-5H-pyrrolo[3',4':3,4]pyrrolo[2,1-a]isoquinoline-3-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / tetrahydrofuran / 24 h / 20 °C

2: N-hydroxyphthalimide; tetraethylammonium bromide / methanol / 12 h / 25 °C / Electrochemical reaction; Green chemistry

With N-hydroxyphthalimide; tetraethylammonium bromide; sodium carbonate; In tetrahydrofuran; methanol;
DOI:10.1039/c9cc04336e