3,8-Dichloro-[1,7]naphthyridine

Base Information

Chemical Name:3,8-Dichloro-[1,7]naphthyridine
CAS No.:1260672-65-8
Molecular Formula:C₈H₄Cl₂N₂
Molecular Weight:199.039
Hs Code.:
Mol file:1260672-65-8.mol

Synonyms:3,8-dichloro-1,7-naphthyridine

Suppliers and Price of 3,8-Dichloro-[1,7]naphthyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3,8-Dichloro-1,7-naphthyridine 95+%
1g
$ 930.00

Anichem
3,8-dichloro-1,7-naphthyridine >95%
1g
$ 950.00

Alichem
3,8-Dichloro-1,7-naphthyridine
1g
$ 919.24

Total 3 raw suppliers

Chemical Property of 3,8-Dichloro-[1,7]naphthyridine

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

3,8-Dichloro-1,7-naphthyridine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,8-Dichloro-[1,7]naphthyridine

There total 7 articles about 3,8-Dichloro-[1,7]naphthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393575-76-2
3-chloro-1,7-naphthyridin-8(7H)-one

: 1260672-65-8
3,8-dichloro-1,7-naphthyridine

Guidance literature:: With trichlorophosphate; at 95 ℃; for 1h;

Reference yield:

: 930303-55-2
2-chloro-1,7-naphthyridin-8(7H)-one

: 1260672-65-8
3,8-dichloro-1,7-naphthyridine

Guidance literature:: In trichlorophosphate;

Reference yield:

: 760207-83-8
3-bromo-5-chloropyridine-2-carbonitrile

: 1260672-65-8
3,8-dichloro-1,7-naphthyridine

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide; hexane; ethyl acetate / 4.25 h / 20 - 50 °C / Inert atmosphere; Sealed tube

2: methanol / 1 h / 55 °C / Sealed tube

3: sodium carbonate; dihydrogen peroxide / water; acetone / 1 h / 20 °C

4: toluene-4-sulfonic acid / benzene / 80 °C / Sonication

5: trichlorophosphate / 1 h / 95 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; sodium carbonate; toluene-4-sulfonic acid; triethylamine; trichlorophosphate; In methanol; hexane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;