1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

Base Information

Chemical Name:1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide
CAS No.:918349-06-1
Molecular Formula:C₂₅H₂₀Cl₃N₃O₄S
Molecular Weight:564.876
Hs Code.:

Synonyms:1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

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Chemical Property of 1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

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Technology Process of 1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

There total 7 articles about 1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033586-98-9
C₂₃H₁₄Cl₄N₂O₃S

: 141-43-5
ethanolamine

: 918349-06-1
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; at 50 ℃; for 1h;

Reference yield:

: 1033586-53-6
N-(4-bromo-2-chlorophenyl)-2,6-dichlorobenzamidine

: 918349-06-1
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrogencarbonate / ethanol / 2.5 h / Heating / reflux

1.2: 1 h / Heating / reflux

2.1: water; potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / 2.5 h / 80 °C

3.1: sodium hydroxide; water / methanol / 2 h / 50 °C

4.1: hydrogenchloride / methanol; water; ethyl acetate

5.1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 1.5 h / 0 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / chloroform / 1 h / 50 °C

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; water; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N,N-dimethyl-formamide; In methanol; 1,2-dimethoxyethane; ethanol; chloroform; water; ethyl acetate; 2.1: Suzuki Coupling;

Reference yield:

: 1033586-55-8
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

: 918349-06-1
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid (2-hydroxyethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 1.5 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / chloroform / 1 h / 50 °C

With oxalyl dichloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In chloroform;