1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

Base Information

Chemical Name:1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid
CAS No.:1033586-55-8
Molecular Formula:C₂₃H₁₅Cl₃N₂O₄S
Molecular Weight:521.808
Hs Code.:

Synonyms:1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

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Chemical Property of 1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

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Technology Process of 1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

There total 5 articles about 1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₁₄Cl₃N₂O₄S^(1-)*Na⁽¹⁺⁾

: 1033586-55-8
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

Guidance literature:: With hydrogenchloride; In methanol; water; ethyl acetate;

Reference yield:

: 1033586-53-6
N-(4-bromo-2-chlorophenyl)-2,6-dichlorobenzamidine

: 1033586-55-8
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / ethanol / 2.5 h / Heating / reflux

1.2: 1 h / Heating / reflux

2.1: water; potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / 2.5 h / 80 °C

3.1: sodium hydroxide; water / methanol / 2 h / 50 °C

4.1: hydrogenchloride / methanol; water; ethyl acetate

With hydrogenchloride; sodium hydroxide; water; sodium hydrogencarbonate; potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In methanol; 1,2-dimethoxyethane; ethanol; water; ethyl acetate; 2.1: Suzuki Coupling;

Reference yield:

: 918350-19-3
1-(4-bromo-2-chlorophenyl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid ethyl ester

: 1033586-55-8
1-(3-chloro-3'-methanesulfonylbiphenyl-4-yl)-2-(2,6-dichlorophenyl)-1H-imidazole-4-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / 2.5 h / 80 °C

2: sodium hydroxide; water / methanol / 2 h / 50 °C

3: hydrogenchloride / methanol; water; ethyl acetate

With hydrogenchloride; sodium hydroxide; water; potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In methanol; 1,2-dimethoxyethane; water; ethyl acetate; 1: Suzuki Coupling;