2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole

Base Information

• Chemical Name: 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole
• CAS No.: 305831-41-8
• Molecular Formula: C₃₇H₃₂N₄
• Molecular Weight: 532.688

Synonyms:2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole

Chemical Property of 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole

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Technology Process of 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole

There total 16 articles about 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-(benzylidene)-p-methylbenzenesulfonamide (51608-60-7) + 5-phenyldipyrromethane (107798-98-1) → 4-methyl-N-(phenyl(5-(phenyl(1H-pyrrol-2-yl)methyl)-1H-pyrrol-2-yl)methyl) benzene sulfonamide (1137951-09-7) + 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole (305831-41-8)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; at 0 ℃;

DOI:10.1016/j.tet.2009.01.009

Reference yield: 55.0%

N-(benzylidene)-p-methylbenzenesulfonamide (51608-60-7) + 5-phenyldipyrromethane (107798-98-1) → 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole (305831-41-8)

Guidance literature:

N-(benzylidene)-p-methylbenzenesulfonamide; With copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; at 20 ℃; for 0.5h;

5-phenyldipyrromethane; In tetrahydrofuran; at 20 ℃;

DOI:10.1002/ejoc.201501062

Reference yield: 35.0%

pyrrole (109-97-7,30604-81-0) + benzaldehyde (100-52-7) → 5-phenyldipyrromethane (107798-98-1) + 5,10-diphenyltripyrrane (195381-16-9) + 2-[phenyl(1H-pyrrol-2-yl)methyl]-5-(phenyl{5-[phenyl(1H-pyrrol-2-yl)methyl]-1H-pyrrol-2-yl}methyl)-1H-pyrrole (305831-41-8)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 2h;

DOI:10.1021/ol006316t

upstream raw materials:

pyrrole

benzaldehyde

5-phenyldipyrromethane

1,9-bis-benzoyl-5-phenyldipyrromethane

Downstream raw materials:

Ph₃CorCo(PPh₃)

5,15,10,20-tetraphenylporphyrin

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