dimesylate of p-hydroxydihydrocinnamyl alcohol

Base Information

• Chemical Name: dimesylate of p-hydroxydihydrocinnamyl alcohol
• CAS No.: 251978-03-7
• Molecular Formula: C₁₁H₁₆O₆S₂
• Molecular Weight: 308.376

Synonyms:dimesylate of p-hydroxydihydrocinnamyl alcohol

Chemical Property of dimesylate of p-hydroxydihydrocinnamyl alcohol

Chemical Property:

Purity/Quality:

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Technology Process of dimesylate of p-hydroxydihydrocinnamyl alcohol

There total 2 articles about dimesylate of p-hydroxydihydrocinnamyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-(4-hydroxyphenyl)propan-1-ol (10210-17-0) + methanesulfonyl chloride (124-63-0) → dimesylate of p-hydroxydihydrocinnamyl alcohol (251978-03-7)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201001402

Reference yield:

4-hydroxyphenylpropionic acid (501-97-3) → dimesylate of p-hydroxydihydrocinnamyl alcohol (251978-03-7)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.201001402

Reference yield: 95.0%

dimesylate of p-hydroxydihydrocinnamyl alcohol (251978-03-7) → methanesulfonic acid 4-(3-azido-propyl)-phenyl ester

Guidance literature:

With sodium azide; In water; N,N-dimethyl-formamide; at 70 ℃; Inert atmosphere;

DOI:10.1002/chem.201001402

upstream raw materials:

3-(4-hydroxyphenyl)propan-1-ol

methanesulfonyl chloride

4-hydroxyphenylpropionic acid

Downstream raw materials:

ethyl (S)-2-methoxy-3-[4-{3-(4-methanesulfonyloxyphenyl)propylamino}phenyl]propionic acid

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