[1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Base Information

Chemical Name:[1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene
CAS No.:182196-52-7
Molecular Formula:C₁₈H₃₂O₂Si₂
Molecular Weight:336.622
Hs Code.:

Synonyms:[1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Suppliers and Price of [1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of [1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of [1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

There total 3 articles about [1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 75-77-4
chloro-trimethyl-silane

: 163799-44-8
1-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-1-phenyl-2-propanone

: 182196-52-7
[1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;
DOI:10.1016/0040-4020(96)00610-2

Reference yield:

: 90-63-1
(RS)-1-hydroxy-1-phenylpropan-2-one

: 182196-52-7
[1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / imidazole / dimethylformamide / 72 h / Ambient temperature

2: 98 percent / LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00610-2

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 182196-52-7
[1-(tert-Butyl-dimethyl-silanyloxy)-2-trimethylsilanyloxy-allyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / imidazole / dimethylformamide / 72 h / Ambient temperature

2: 98 percent / LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00610-2