(1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

Base Information

Chemical Name:(1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane
CAS No.:78174-32-0
Molecular Formula:C₁₁H₂₀ClNO₃
Molecular Weight:249.738
Hs Code.:

Synonyms:(1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

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Chemical Property of (1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

Chemical Property:

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Technology Process of (1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

There total 4 articles about (1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16844-21-6
N-Chlorourethan

: 19096-89-0
methoxymethylenecyclohexane

: 78174-32-0
(1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

: 78174-31-9
1-ethoxycarbonylaminocyclohexanecarboxaldehyde dimethyl acetal

Guidance literature:: With sodium methylate; Yield given. Multistep reaction. Yields of byproduct given; 1.) irradiation, CH₂Cl₂, -70 degC; 2.) methanol, -70 degC, then allowed to warm to r.t.;

Reference yield:

: 67-56-1
methanol

: 16844-21-6
N-Chlorourethan

: 19096-89-0
methoxymethylenecyclohexane

: 78174-32-0
(1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

: 78174-31-9
1-ethoxycarbonylaminocyclohexanecarboxaldehyde dimethyl acetal

Guidance literature:: With chromium dichloride; In chloroform; at -78 ℃; Product distribution; the regiochemistry of the radical addition of N-chloroamides to various enol ethers;
DOI:10.1016/S0040-4020(01)88026-1

Reference yield:

: 16844-21-6
N-Chlorourethan

: 19096-89-0
methoxymethylenecyclohexane

: 78174-33-1
(1-Formyl-cyclohexyl)-carbamic acid ethyl ester

: 78174-32-0
(1'-chlorocyclohexyl)-ethoxycarbonylaminomethoxymethane

: 78174-31-9
1-ethoxycarbonylaminocyclohexanecarboxaldehyde dimethyl acetal

Guidance literature:: With water; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, ir., -70 deg C;
DOI:10.1016/S0040-4020(01)88026-1