(phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate

Base Information

• Chemical Name: (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate
• CAS No.: 1633750-72-7
• Molecular Formula: C₄₄H₃₆F₃IO₃SSi
• Molecular Weight: 856.819

Synonyms:(phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate

Chemical Property of (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate

Chemical Property:

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Technology Process of (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate

There total 3 articles about (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,3-bis(trimethylsilyl)-5,6,7,8-tetraphenylnaphthalene + [bis(acetoxy)iodo]benzene (3240-34-4) + sodium triflate (2926-30-9) → (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate (1633750-72-7)

Guidance literature:

2,3-bis(trimethylsilyl)-5,6,7,8-tetraphenylnaphthalene; [bis(acetoxy)iodo]benzene; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 0.5h;

sodium triflate; In dichloromethane; water;

DOI:10.1002/adsc.201400081

Reference yield:

1,2,4,5-tetrakis(trimethylsilyl)benzene (17156-61-5) → (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate (1633750-72-7)

Guidance literature:

Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 0 °C

2: tetrabutyl ammonium fluoride / dichloromethane; tetrahydrofuran / 0.33 h / 20 °C

3: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 20 °C

With boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/adsc.201400081

Reference yield:

(phenyl)[2,4,5-tris(trimethylsilyl)phenyl]iodonium triflate (1026471-76-0) → (phenyl)(3-trimethylsilyl-5,6,7,8-tetraphenyl-2-naphthalen-yl)iodonium triflate (1633750-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / dichloromethane; tetrahydrofuran / 0.33 h / 20 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 20 °C

With boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/adsc.201400081

upstream raw materials:

[bis(acetoxy)iodo]benzene

sodium triflate

1,2,4,5-tetrakis(trimethylsilyl)benzene

(phenyl)[2,4,5-tris(trimethylsilyl)phenyl]iodonium triflate

Downstream raw materials:

1,4-dihydro-5,6,7,8-tetraphenyl-1,4-epoxyanthracene

1,2,3,4,5,6,7,8-octaphenylanthracene

1,5,6,7,8-pentaphenyl-1H-naphtho[2,3-d]triazole

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