Technology Process of C19H34N2O3SSi
There total 8 articles about C19H34N2O3SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N-<(benzyloxy)carbonyl>-2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine;
With
palladium on activated charcoal; hydrogen;
In
ethanol;
4-Nitrobenzenesulfonyl chloride;
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
With
palladium on activated charcoal; hydrogen;
In
ethanol;
under 2068.65 Torr;
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethanol;
for 3h;
under 2068.65 Torr;
DOI:10.1021/jm201699w
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium carbonate / water; acetone / 0 °C
2: 1H-imidazole / N,N-dimethyl-formamide
3: palladium on activated charcoal; hydrogen / ethanol / 3 h
4: N-ethyl-N,N-diisopropylamine / dichloromethane
5: palladium on activated charcoal; hydrogen / ethanol / 3 h / 2068.65 Torr
With
1H-imidazole; palladium on activated charcoal; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm201699w