Technology Process of C27H35NO5
There total 4 articles about C27H35NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 14 percent / diethyl ether / 1.) 0 deg C 1 h: 2.) 3 h room temperature
2: 68 percent / bromine / dioxane / 2 h
3: 88 percent / sodium borohydride / dioxane; H2O / 1.) 2 h at 5 deg C; 2.) 30 min room temperature
4: 78 percent / 10 percent aq potassium carbonate / dioxane / 17 h / Heating; in the dark
5: 70 percent / p-toluenesulfonic acid / benzene / 24 h / Heating; in the dark
With
sodium tetrahydroborate; bromine; potassium carbonate; toluene-4-sulfonic acid;
In
1,4-dioxane; diethyl ether; water; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 68 percent / bromine / dioxane / 2 h
2: 88 percent / sodium borohydride / dioxane; H2O / 1.) 2 h at 5 deg C; 2.) 30 min room temperature
3: 78 percent / 10 percent aq potassium carbonate / dioxane / 17 h / Heating; in the dark
4: 70 percent / p-toluenesulfonic acid / benzene / 24 h / Heating; in the dark
With
sodium tetrahydroborate; bromine; potassium carbonate; toluene-4-sulfonic acid;
In
1,4-dioxane; water; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / 10 percent aq potassium carbonate / dioxane / 17 h / Heating; in the dark
2: 70 percent / p-toluenesulfonic acid / benzene / 24 h / Heating; in the dark
With
potassium carbonate; toluene-4-sulfonic acid;
In
1,4-dioxane; benzene;
