(3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

Base Information

Chemical Name:(3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate
CAS No.:1034026-57-7
Molecular Formula:C₂₂H₁₈Cl₂O₃
Molecular Weight:401.289
Hs Code.:

Synonyms:(3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

Chemical Property:

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Technology Process of (3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

There total 1 articles about (3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-22-3
2-methyl-5-hydroxybenzoic acid

: 766-80-3
1-bromomethyl-3-chlorobenzene

: 1034026-57-7
(3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 80 ℃;

Reference yield:

: 1034026-57-7
(3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

: 1034026-16-8
5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoic acid

Guidance literature:: (3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate; With lithium hydroxide; water; In 1,4-dioxane; at 20 ℃;

With hydrogenchloride; water; In diethyl ether; Product distribution / selectivity;

Reference yield:

: 1034026-57-7
(3-chlorophenyl)methyl 5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoate

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: water; lithium hydroxide / 1,4-dioxane / 20 °C / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

3: triethylamine / dichloromethane / 20 °C

4: hydrogenchloride; water; acetic acid / 2 h / 90 °C

With hydrogenchloride; oxalyl dichloride; water; acetic acid; triethylamine; N,N-dimethyl-formamide; lithium hydroxide; In 1,4-dioxane; dichloromethane;