ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Base Information

Chemical Name:ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate
CAS No.:1034026-35-1
Molecular Formula:C₂₆H₂₆ClNO₄
Molecular Weight:451.95
Hs Code.:

Synonyms:ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

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Chemical Property of ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

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Technology Process of ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

There total 9 articles about ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-22-3
2-methyl-5-hydroxybenzoic acid

: 1034026-35-1
ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C

2: water; lithium hydroxide / 1,4-dioxane / 20 °C / Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 20 °C

With oxalyl dichloride; water; potassium carbonate; triethylamine; N,N-dimethyl-formamide; lithium hydroxide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1034026-58-8
5-{[(3-chlorophenyl)methyl]oxy}-2-methylbenzoyl chloride

: 50712-56-6
ethyl 2-(4-amino-3-methylphenyl)acetate

: 1034026-35-1
ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 - 30 ℃; for 14.17 - 14.25h; Product distribution / selectivity;

Reference yield:

: 1028543-03-4
ethyl phenylmethyl [3-methyl-4-nitrophenyl]propanedioate

: 1034026-35-1
ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr

2: triethylamine / dichloromethane / 20 °C

With hydrogen; triethylamine; palladium 10% on activated carbon; In ethanol; dichloromethane;