1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

Base Information

Chemical Name:1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate
CAS No.:156022-73-0
Molecular Formula:C₂₁H₃₈N₂O₃Si
Molecular Weight:394.63
Hs Code.:

Synonyms:1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

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Chemical Property of 1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

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Technology Process of 1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

There total 4 articles about 1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 180285-08-9
1,1-dimethylethyl (R)-2,5-diaza-7-hydroxy-6-phenylheptanoate

: 156022-73-0
1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1055/s-1996-4299

Reference yield:

: 4530-20-5
BOC-glycine

: 156022-73-0
1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / DCC / CH₂Cl₂ / 7 h / 0 - 20 °C

2: 94 percent / LiAlH₄ / diethyl ether / 24 h / Ambient temperature

3: 80 percent / imidazole / dimethylformamide / 18 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1996-4299

Reference yield:

: 56613-80-0
D-2-phenylglycinol

: 156022-73-0
1,1-dimethylethyl (R)-2,5-diaza-9,9,10,10-tetramethyl-8-oxa-6-phenyl-9-silaundecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / DCC / CH₂Cl₂ / 7 h / 0 - 20 °C

2: 94 percent / LiAlH₄ / diethyl ether / 24 h / Ambient temperature

3: 80 percent / imidazole / dimethylformamide / 18 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1996-4299