Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

Base Information

Chemical Name:Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane
CAS No.:87170-97-6
Molecular Formula:C₂₁H₃₂OS₃Si
Molecular Weight:424.768
Hs Code.:

Synonyms:Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

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Chemical Property of Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

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Technology Process of Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

There total 1 articles about Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 80398-85-2
1-Phenylsulfanyl-3-oxa-bicyclo[3.1.0]hexan-2-ol

: C₁₉H₂₂LiOPS₂

: 87170-97-6
Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

Guidance literature:: Yield given. Multistep reaction;

Reference yield: 95.0%

: 87170-97-6
Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

: Trimethyl-[(1Z,4E)-7-(2-methyl-[1,3]dithian-2-yl)-4-phenylsulfanyl-hepta-1,4-dienyloxy]-silane

Guidance literature:: at 600 ℃; under 0.005 Torr;

Reference yield:

: 87170-97-6
Trimethyl-{2-[(E)-3-(2-methyl-[1,3]dithian-2-yl)-propenyl]-2-phenylsulfanyl-cyclopropylmethoxy}-silane

: 69854-98-4
7-E,9-Z methyl trisporate B

Guidance literature:: Multi-step reaction with 8 steps

1: 95 percent / 600 °C / 0.01 Torr

2: 68 percent / (CH₃O)3CH, HCl / -10 - 0 °C

3: 75 percent / (dppp)NiCl₂ / tetrahydrofuran; diethyl ether / Heating

4: 100 percent / HCl, H₂O / acetonitrile / Ambient temperature

5: 94 percent / tetrahydrofuran / -78 °C

8: 22 percent / PhCH₂N(CH₃)3(+)*OCH₃(-) / methanol / -10 - 0 °C

With hydrogenchloride; bis(triphenylphosphine)nickel(II) chloride; water; benzyltrismethylammonium methoxide; trimethyl orthoformate; In tetrahydrofuran; methanol; diethyl ether; acetonitrile;